中温固体比热容测量基准的研究进展

doi:10.3969/j.issn.1000-1158.2016.04.11

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Abstract The primary heat capacity standard for medium temperature is employed for the traceability of the specific heat capacity, phase transition temperature and enthalpy. The device mainly adopts the adiabatic calorimetric method, which makes the calorific value traceable to SI units. Firstly, the research significance and the principle of primary heat capacity standard is introduced, and then the progress on the research in the field is demonstrated. Finally new design and scheme of primary heat capacity standard based on this work are put forward.

Key words： metrology heat capacity primary standard adiabatic calorimetry phase transition

Received: 14 August 2015 Published: 31 May 2016

PACS:

TB94

Fund:Research and establishment of adiabatic calorimeter for measuring the specific heat capacity from 300 to 550K

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	Articles by authors
	LI Jia
	WANG Can
	WANG Hai-feng
	SUN Guo-hua

Cite this article:

LI Jia,WANG Can,WANG Hai-feng, et al. Research Progress of Primary Heat Capacity Standard for Medium Temperature[J]. Acta Metrologica Sinica, 2016, 37(4): 384-389.

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http://jlxb.china-csm.org:81/Jwk_jlxb/EN/10.3969/j.issn.1000-1158.2016.04.11 OR http://jlxb.china-csm.org:81/Jwk_jlxb/EN/Y2016/V37/I4/384

［1］蔡岸,谢华清,奚同庚.航天器用十一种热控材料热物理性质及其与显微组织和工艺因素关系的研究［J］.无机材料学报,2006,21(5):1173-1178.
［2］王百亚,王秀云,张炜.一种航天器用外热防护涂层材料研究［J］.固体火箭技术,2005,28(3):216-227.
［3］李兴刚,张利军,胡润芝,等. 一种耐高焓低热流环境隔热材料［J］.宇航材料工艺,2014,44(3):62-66.
［4］罗义英,牛志荣,杨学宾.泡沫玻璃外墙外保温系统的热物性参数研究［J］.新型建筑材料,2011,38(5): 50-52.
［5］查世彤,马一太,魏东.食品热物性的研究与比较［J］.工程热物理学报,2001,22(3): 275-277.
［6］王补宣,江亿. 用热探针法现场测试松散介质的热物性的原理性误差［J］. 计量学报, 1986,7(3):159-167.
［7］杨长生,马沛生,夏淑倩.DSC法测定醋酸-水溶液的比热［J］.高校化学工程学报,2002,16(5): 479-483.
［8］葛山,尹玉成,刘志强,等.高炉炭砖导热系数的测定［J］.炼铁,2008,27（2）:47-49.
［9］葛山,尹玉成. 激光闪光法测定耐火材料导热系数的原理与方法［J］.理化检验-物理分册,2008,44（2）:75-78.
［10］张金涛,原遵东,邱萍,等.高精密自动绝热量热计［J］.计量学报,2005,26（4）:320-325.
［11］张金涛,孙建平,邱萍,等.高精密自动绝热量热装置［J］.计量技术,2005,（4）:8-10.
［12］Bessergenev V G , Kovalevskaya Y A, Paukov I E, et al. Heat capacity measurements under continuous heating and cooling using vacuum adiabatic calorimetry［J］.Thermochimica Acta,1989,139(1): 245-256.
［13］Eric F L, Joseph F M, Roger E,et al. Progress in International Research on Thermodynamic and Transport Properties［M］.New York:Academic Press,1962.
［14］Oetting F L, West E D. An adiabatic calorimeter for the range 300 to 700K［J］. Chemical Thermodynamics,1982,14(2): 107–114.
［15］Ginnings D C, West E D. Principles of Calorimetric Design［J］. Experimental Thermodynamics, 1968, 1:85-131.
［16］Armstrong L D, Grayson-Smith H. High Temperature Calorimetry［J］. Canadian Journal of Research,1950,28(A):51-59.
［17］West E D. The Heat Capacity of Sulfur from 25 to 450 ℃,the Heats and Temperatures of Transition and Fusion［J］. American Chemical Society,1959,81:29-37
［18］Dole M, Hettinger W P, Larson J N, et al. Calorimetry of High Polymers.I.Automatic Temperature Recording and Control of Adiabatic Jacket［J］. The Review of Scientific Instruments,1951,22(11):812-817.

［19］West E D, Westrum E F. Adiabatic Calorimetry From 300 to 800°K［J］. Experimental Thermodynamics, 1968,1:333-367.
［20］Inaba A. An adiabatic calorimeter for use at intermediate and higher temperatures the heat capacity of synthetic sapphire (α-Al2O3) from 70 to 700K［J］.Chemical Thermodynamics,1983,15(12): 1137-1143.
［21］Michio Sorai, Kazutoshi Kaji, Yuki Kaneko. An automated adiabatic calorimeter for the temperature range 13K to 530K The heat capacities of benzoic acid from 15K to 305K and of synthetic sapphire from 60K to 505K［J］. Chemical Thermodynamics,1992,24(2): 167-180.
［22］谭志诚,张际标,孟霜鹤,等.70～580K小样品全自动精密绝热量热装置的建立［J］.中国科学,1999,29（2）:162-168.
［23］谭志诚,刘北平,颜君彪,等.一种新型80～400K高精度全自动绝热量热系统的建立［J］.计算机与应用化学,2003,20（3）:264-268.