|
|
Development of Vitamin B1 Standard Reference Material in Multivitamin Tables |
TIAN Ying1,2,YANG Yi1,HUANG Ting2,LIU Jun2 |
1. Beijing University of Chemical Technology, Beijing 100029, China
2. National Institute of Metrology, Beijing 100013, China |
|
|
Abstract A new standard reference material of vitamin B1 in multivitamin tables is developed. The sample preparation involves an acid extraction and centrifugation, LC-IDMS method and LC-UV method verify its value. The method is validated by standard reference material SRM 3280, and accuracy of analysis result is validated by two laboratories further. The standard value of vitamin B1 in multivitamin tables is 2.76mg/g and the expanded uncertainty is 0.22mg/g (k=2).
|
|
|
|
|
|
[1]全浩,韩永志. 标准物质及其应用技[M].中国标准出版社,2002.
[2]JJG 1006—94, 一级标准物质[ S] .
[3]李云巧,崔婷,王道. 磷溶液标准物质的研制[J].计量学报,2006,27(1):77-80.
[4]Huang T, Zhang W, Liu J, et al. A new certified reference material (GBW10037) of vitamin B3 in infant formula[J]. J Food Compos Anal,2010,23(4):367-372. |
|
|
|